Equilibrium between titanium ions and high-purity titanium elect...

TiClx (x = 2.17) was prepared by using titanium sponge to reduce the concentration of TiCl4 in a NaCl.KCl melt under negative pressure. The as-prepared NaCl.KCl.TiClx melt was employed as the electrolyte, and two parallel crude titanium plates and one hig