The crystals of enantiopure SS-[cis-Rh2(Ph2C6H4)2(O2CC2F4CO2)]2((CH3)2CHCH2NH2)3(1) were obtained from the reaction of S-[cis-Rh2(Ph2C6H4)2(CH3CN)6]BF4 (S-2) and(Et4N)2(O2CC2F4CO2) in CH2Cl2/CH3OH under the presence of sec-butyl amine. Compound 1 crystall
