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HKL CHANNEL5-EBSD使用手册
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The CHANNEL 5 suite of programs has been developed to allow you, the user, to manipulate, analyse and display Electron Backscatter Diffraction (EBSD) data with comparative ease. The programs have been designed to be as flexible and extendible as possible and to allow several users to work independently or together on the same computer or over a network.
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HKL Technology
CHANNEL 5
HKL Technology
HKL Technology ApS HKL Technology, Inc.
Address:
HKL Technology ApS,
Majsmarken1
9500 Hobro
Denmark
HKL Technology, Inc.
52A Federal Road, Unit 2D,
Danbury, CT 06810,
United States
Contact Niels-Henrik Schmidt Tim Maitland
Telephone: +45 96 57 26 00 [1] 203 748 3757
Fax: +45 96 57 26 09 [1] 203 748 0360
Info: info@hkltechnology.com
Support: support@hkltechnology.com
Important Information
Product Development
HKL Technology continuously develop their products in line with
technological advancements and reserve the right to change the design
and specification of their products without prior notice. Although every
care has been taken in the preparation of this document, HKL
Technology cannot accept liability for damage or injury resulting from its
use. If users are unsure of any of the information presented in this
document, particularly with reference to safety issues, they must contact
HKL Technology prior to undertaking any instructions.
Copyright Information
© HKL Technology 2003. All rights reserved. No part of this publication
may be reproduced, stored in a retrieval system or transmitted in any
form or by any means without the prior written permission of HKL
Technology
Release date: January 2003
Author Information
This manual was written by Austin Day and Pat Trimby, with assistance
from Klaus Mehnert and Berndt Neumann.
Please report omissions/errors to support@hkltechnology.com
HKL Technology CHANNEL 5
HKL Technology CHANNEL 5 Contents •
••
• i
Contents
General Introduction 1.1
The CHANNEL 5 suite of programs....................................................................1.1
Software flexibility and integration.........................................................1.3
User network, meetings and support.......................................................1.3
Installing the CHANNEL 5 software...................................................................1.4
Offline installation ..................................................................................1.5
Online Installation...................................................................................1.6
HASP copy protection.............................................................................1.7
Computer specification ...........................................................................1.8
Uninstalling CHANNEL 5......................................................................1.8
Working with Windows.......................................................................................1.8
CHANNEL 5 - keyboard shortcuts ......................................................................1.9
The manuals and help file ..................................................................................1.10
Inkling ................................................................................................................1.11
Contacting HKL Technology.............................................................................1.12
Twist - diffraction data creator 2.1
Chapter Overview ................................................................................................2.1
Useful sources of Crystal data..............................................................................2.2
Running Twist ......................................................................................................2.2
The Twist Toolbar................................................................................................2.3
Using Twist..........................................................................................................2.3
Creating a new Crystal.........................................................................................2.4
Entering crystallographic data.................................................................2.4
Entering Atom data .................................................................................2.5
Saving a Crystal to a CRY file................................................................2.6
Reading a CRY file in to Twist............................................................................2.7
Converting a Laue group to a Space group.............................................2.7
Reflector Intensity Calculations...........................................................................2.8
Structure Factor Calculations..................................................................2.9
Calculating reflector intensities...............................................................2.9
Saving Reflectors to an HKL file..........................................................2.10
Example: Dolomite ............................................................................................2.11
Choosing the correct Space Group........................................................2.11
Adding Atoms for Dolomite .................................................................2.12
Viewing Wyckoff formulae ...............................................................................2.14
Example: Clinopyroxene....................................................................................2.15
Choosing the correct Space Group........................................................2.16
Adding Atoms for Clinopyroxene.........................................................2.16
Indexing a Clinopyroxene EBSP ..........................................................2.17
Unit Cell Simulation ..........................................................................................2.18
Flamenco - an Introduction 3.1
Overview..............................................................................................................3.1
ii •
••
• Contents HKL Technology CHANNEL 5
User and EBSD requirements................................................................. 3.2
Your EBSD System.............................................................................................3.2
Introducing Flamenco.......................................................................................... 3.3
Starting Flamenco................................................................................................ 3.4
Managing The Layout..........................................................................................3.5
Docking and Undocking Windows......................................................... 3.6
Setting up the workspace........................................................................ 3.7
The Cycle Control Window.................................................................... 3.8
The Match Units window .......................................................................3.9
User Profiles ...................................................................................................... 3.10
Specimen Preparation........................................................................................3.10
Introduction .......................................................................................... 3.10
Setting up your SEM .........................................................................................3.12
Positioning the specimen in the SEM................................................... 3.12
Configuring the SEM for EBSD...........................................................3.12
Flamenco - Imaging 4.1
Overview ............................................................................................................. 4.1
Starting the imaging system.................................................................................4.3
Acquiring an image..............................................................................................4.4
Setting up the SEM................................................................................. 4.4
Scanning ................................................................................................. 4.4
Enhancing...............................................................................................4.5
Focusing..................................................................................................4.5
Changing the image size......................................................................... 4.6
Adding a comment.................................................................................. 4.6
Tilt Correction and Magnification.......................................................... 4.7
Saving and exporting images............................................................................... 4.8
Using an image for subsequent EBSD analyses .................................................. 4.9
Calibrating the imaging system ........................................................................... 4.9
Loading a sample for calibration............................................................4.9
Calibrating the geometry ...................................................................... 4.10
Calibrating the magnification ...............................................................4.11
Checking the Calibration......................................................................4.12
Working without an imaging system................................................................. 4.14
Flamenco - EBSD Acquisition 5.1
Overview ............................................................................................................. 5.1
EBSD Measurements - An Outline......................................................................5.3
Acquisition Pages in Flamenco ...........................................................................5.3
Frozen SEM Image................................................................................. 5.4
Live EBSP .............................................................................................. 5.6
EBSP Geometry...................................................................................... 5.7
Band Detection ....................................................................................... 5.8
Solution................................................................................................. 5.10
EBSP production ............................................................................................... 5.15
Switching on......................................................................................... 5.15
EBSD Background correction .............................................................. 5.16
Using the Argus 20............................................................................... 5.16
Nordlys EBSD Detector .................................................................................... 5.20
Description of detector .........................................................................5.20
Connection instructions ........................................................................ 5.20
Endstops................................................................................................5.20
Using the Nordlys handset.................................................................... 5.21
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